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47, 1576 (1982). 5-11 P. Schiess, S. Rutschmann and V. V. , 23, 3665, 3669 (1982); K. , Chem. , 1697 (Ϊ982). Cl 1) Mg, THF f^Yi 2) E + ^^^^ 38-82% Starting Benzocyclobutene in two steps from 2-methyl benzaldehydes. 5-12 H. Kropf and F. Angi, J. Chem. Res ( S h 136 (1982); K. Schlogl and W. Weissensteiner, Synthesis, 50 (1982). 5-13 R. B. Bates and C. A. Ogle, J. Org. , 47, 3949 (1982); D. Wilhelm, T. Clark and P. v. R. , 23, 4077 (1982). CHpCHo τ IP 1) nBuLi, ΚΟ Βιι I I 2) Me 2 S0 4 3) nBuLi, K O ^ u Crl^CHoCHo 4) Et 2 S0 4 74% Also, reactions of dianions of xylenes.

H. Clark and D. G. Cork, Chem. , 635 (1982); C. , Liebigs Ann. Chem,, 1173 (1982). a„la-4 T. , Chem. , 353, 1291, 1441, 1459, 1903 (1982); S. Shenvi and J. K. , 23, 627 (1982). la-5 Y· Yamamoto, H. , Bull. Chem. Soc. , 55, 1907 (1982); D. L. J. Clive, C. G. Russell and S. C. Suri, J. Org. , 47, 1632 (1982). Me03SiO OH 0 6 1 1) nBuLi, THF II f ^γ^Φ ^*. a„la-6 Y. Yamamoto and K. Maruyama, J. Amer. Chem. S o c , 104, 2323 (1982). la-7 J. Hooz and J. Oudenes, Synth. , 12. 189 (1982); H. Hamana and T.

Janssen, L. H. J. G. Simons and E. F. Godefroi, Synthesis, 389 (1982); J. Drouin and J. M. Conia, Synth. , J2_, 81 (1982). tf SiMe. lb-4 2190 (1982); F. , J. Amer. Chem. S o c , 104, J. Org. , 47, 4254 (1982). lb-5 S. D. , J. Amer. Chem. S o c . 104. 872 (1982); J. Org. , 47, 1349 (1982). CHO TiCl, CHO TAMA*, THF -35°C 50% TAMA = N-Methylanilinium Trifluoroacetate. lb-6 M. E. , Tetrahedron, 38, 2279 (1982); T. Yoshida and S. Saito, Bull. Chem. Soc. , 55, 3931 (1982). NaH, THF RT 73% (Retroaldol-Aldol) I .

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