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3 1 , 443, 454 ( 1 9 8 3 ) . 0 " 1 -C-R 1 1) LDA, THF S-CH 2 -R 2 2 ) A ^· NH 4C1 . 2-5 K. F u j i , M. Ueda and E. F u j i t a , Chem. , 49 ( 1 9 8 3 ) ; J . Thiem e t a l . , Liebigs Ann. , 2185 ( 1 9 8 3 ) . 2-6 M. Rosenberger, N. , J. Am. Chem. S o c , 105, 3656, 3661 (1983); B. , Synthesis, 628 (Ϊ983); M. H. H. Nkunya and B. Zwanenburg, Rec. Trav. , 102, 461 (1983); F. Fischer and P. PalitzschTJ. Prakt. , 325", 835 (1983). φ-^Ό 0HC(CH2)3C02Me R Br » Aq. NaOH, CH2C12 ^ H - ^ V ^ > ^ ( C H 2 ) 3C02Me R· 72% I .

R. Barton, W. B. Motherwell and S. Z. Zaid, Bull. Soc. Chim. Fr. I I , 61 (1983); T. Fujisawa, Y. Kurita and T. Sato, Chem. L e t t . , 1537 (1983). R1. 9 R^ CH-N09 R,CH0 —». 2-2 K. S. Petrakis, G. Batuand J . Fried, Tetrahedron L e t t . , 24, 3063 (1983); G. Rosini, R. Ballini and P. Sorrenti, Tetrahedron, 39, 4127 (1983). 2-3 S. , 24, 3927, (1983); A. de Groot and B. J. M. Jansen, Synth. , 13, 985 (1983). 2-4 Y. Ohtsuka and T. O i s h i , Chem. Pharm. B u l l . , 3 1 , 443, 454 ( 1 9 8 3 ) .

Coutrot, J. R. Dormoy andTT Moukimou, J. Organometal. , 258, C25 (1983). 3-2 E. E. Aboujaoude, N. Collignon and P. Savignac, Synthesis, 634 (1983); K. C. Tang and J. K. Coward, J. Org. , 48, 5001 (1983); H. J. Bestmann, K. Kumar and L. Kisielowski, Chem. , 116, 2378 (1983); L. Capuano, T. Triesch and A. Wilimes, ibid, 116, 3767 (1983). , S ^R2 (ROkPCH X R J 1) nBuLi , S ? 3-3 E. J. Corey and T. M. , 24, 3163 , 3165 (1983). Bu0CH* 1) s-BuLi r ^ *BuOCH,E ά KO^Bu .

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